Methanesulfonic acid, 1,1,1-trifluoro-, bis(1,1-dimethylethyl)(2-methylpropyl)silyl ester - Names and Identifiers
Methanesulfonic acid, 1,1,1-trifluoro-, bis(1,1-dimethylethyl)(2-methylpropyl)silyl ester - Physico-chemical Properties
Molecular Formula | C13H27F3O3SSi
|
Molar Mass | 348.5 |
Density | 1.25 |
Boling Point | 100-101°C / 1 |
Specific Gravity | 1.25 |
Storage Condition | Room Temprature |
Sensitive | 7: reacts slowly with moisture/water |
Methanesulfonic acid, 1,1,1-trifluoro-, bis(1,1-dimethylethyl)(2-methylpropyl)silyl ester - Introduction
Di-tert-butyl isobutyl silyl trifluoromethanesulfonic acid is an organosilicon compound, also known as TBDMDA. The following is an introduction to its nature, use, preparation and safety information:
Properties: Di-tert-butyl isobutyl methyl silyl trifluoromethanesulfonic acid is a colorless to light yellow liquid with low surface tension and volatility. It can be dissolved in many organic solvents at room temperature, such as ethanol, acetone and dimethylformamide.
Uses: TBDMDA is widely used as a catalyst and crosslinking agent in organic synthesis. It can be used to catalyze olefin polymerization reactions, oxidation reactions, esterification and etherification reactions. In addition, it can also be used as a crosslinking agent for coatings and sealing materials, and can also be used to prepare high-performance resins and adhesives.
Preparation method: The preparation of di-tert-butyl isobutyl methyl silyl trifluoromethanesulfonic acid can be obtained by fluorination and sulfonation reaction of silane. First, di-tert-butyl isobutyl silane is reacted with boron trifluoride to produce di-tert-butyl isobutyl silyl trifluoromethane borate. This ester is then reacted with a sulfonic acid to yield the final product, TBDMDA.
Safety information: During use and storage, be careful to avoid contact with skin and eyes, and ensure that you operate in a well-ventilated place. Since di-tert-butyl isobutyl methyl silyl trifluoromethanesulfonic acid is organic and may have some health effects, it is necessary to follow appropriate laboratory practices.
Last Update:2024-04-09 21:04:16